[Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆

Base Information

Chemical Name:[Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆
CAS No.:583884-55-3
Molecular Formula:C₃₈H₄₁P₂Ru*F₆P
Molecular Weight:805.725
Hs Code.:

[Ru(=C=CH<sub>2</sub>)(1,2-bis(diphenylphosphino)ethane)Cp*]PF<sub>6</sub>

Synonyms:

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Chemical Property of [Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆

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Technology Process of [Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆

There total 1 articles about [Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: ammonium hexafluorophosphate

: pentamethylcyclopentadienyl(1,2-bis(diphenylphosphino)ethane)chlororuthenium(II)

: 1066-54-2
trimethylsilylacetylene

: 583884-55-3
[Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆

Guidance literature:: In methanol; under N2, Schlenk technique; adding HCCSiMe3 to suspn. of RuCl(dppe)Cp* and NH4PF6 in methanol; heating at reflux for 1 h; cooling to room temp.; filtration on sintered glass frit; washing with Et2O; drying solid undervac.; elem. anal.;
DOI:10.1021/om030015g

Reference yield: 95.0%

: 583884-55-3
[Ru(=C=CH₂)(1,2-bis(diphenylphosphino)ethane)Cp*]PF₆

: 670-54-2
ethenetetracarbonitrile

: 1112299-03-2
Ru{C≡CC(CN)=C(CN)₂}(dppe)Cp*

Guidance literature:: With CH₃Li; In tetrahydrofuran; hexane; (N2) a soln. of complex in THF at -78°C was treated with CH3Li inhexane, after 25 min tetracyanoethene was added, warmed to room temp., stirred overnight; the solvent was removed, preparative TLC; elem. anal.;
DOI:10.1021/om2007503