2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate

Base Information

Chemical Name:2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate
CAS No.:900151-11-3
Molecular Formula:C₃₅H₃₉O₇P
Molecular Weight:602.664
Hs Code.:

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Chemical Property of 2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate

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Technology Process of 2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate

There total 3 articles about 2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: dibenzyl ethylphosphonic acid

: 284036-78-8
2,3,5-tri-O-benzyl-β-D-ribofuranosyl trichloroacetimidate

: 2,3,5-tri-O-benzyl-β-D-ribofuranosyl benzyl ethylphosphonate

: 900151-11-3
2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate

Guidance literature:: With 4 A molecular sieve; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1139/V06-038

Reference yield:

: 4537-62-6
dibenzyl ethylphosphonate

: 900151-11-3
2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.87 g / 1,4-diazabicyclo[2.2.2]octane / toluene / 3 h / Heating

2: molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 0 - 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; 4 A molecular sieve; In dichloromethane; toluene;
DOI:10.1139/V06-038

Reference yield:

: 89361-52-4
2,3,5-tris-O-(phenylmethyl)-β-D-ribofuranose

: 900151-11-3
2,3,5-tri-O-benzyl-α-D-ribofuranosyl benzyl ethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / CH₂Cl₂ / 20 °C

2: molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 0 - 20 °C

With 4 A molecular sieve; potassium carbonate; In dichloromethane;
DOI:10.1139/V06-038