Technology Process of C42H57NO10Si
There total 8 articles about C42H57NO10Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 90 percent / [(o-tol)3P]2PdCl2 / tetrahydrofuran; N,N-dimethyl-acetamide / ultrasonification
2: 82 percent / DMAP / acetonitrile
3: 96 percent / OsO4; N-methylmorpholine N-oxide; H2O / 2-methyl-propan-2-ol
4: 82 percent / DMSO; py*SO3; Et3N / CH2Cl2
5: 100 percent / NaClO2; KH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O
6: Et3N / dimethylformamide
With
dmap; sodium chlorite; potassium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; water; sulfur trioxide pyridine complex; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine;
[(o-tol)3P]2PdCl2;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-2006-950399
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 82 percent / imidazole / tetrahydrofuran
2: 90 percent / [(o-tol)3P]2PdCl2 / tetrahydrofuran; N,N-dimethyl-acetamide / ultrasonification
3: 82 percent / DMAP / acetonitrile
4: 96 percent / OsO4; N-methylmorpholine N-oxide; H2O / 2-methyl-propan-2-ol
5: 82 percent / DMSO; py*SO3; Et3N / CH2Cl2
6: 100 percent / NaClO2; KH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O
7: Et3N / dimethylformamide
With
1H-imidazole; dmap; sodium chlorite; potassium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; water; sulfur trioxide pyridine complex; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine;
[(o-tol)3P]2PdCl2;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-2006-950399
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 82 percent / imidazole / tetrahydrofuran
2: 90 percent / [(o-tol)3P]2PdCl2 / tetrahydrofuran; N,N-dimethyl-acetamide / ultrasonification
3: 82 percent / DMAP / acetonitrile
4: 96 percent / OsO4; N-methylmorpholine N-oxide; H2O / 2-methyl-propan-2-ol
5: 82 percent / DMSO; py*SO3; Et3N / CH2Cl2
6: 100 percent / NaClO2; KH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O
7: Et3N / dimethylformamide
With
1H-imidazole; dmap; sodium chlorite; potassium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; water; sulfur trioxide pyridine complex; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine;
[(o-tol)3P]2PdCl2;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-2006-950399