Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl

Base Information

Chemical Name:Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl
CAS No.:922171-28-6
Molecular Formula:C₃₆H₂₃ClN₂Pt
Molecular Weight:714.125
Hs Code.:

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Chemical Property of Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl

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Technology Process of Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl

There total 1 articles about Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 321882-19-3
1,3-bis(4'-phenyl-2'-quinolinyl)benzene

: 922171-28-6
Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl

Guidance literature:: In acetic acid; (under N2, Schlenk); ligand and K2PtCl4 added to acetic acid, mixt. heated at 100-120°C, refluxed for 72 h, cooled to ambient temp.; ppt. filtered, washed with MeOH and Et2O, recrystd. from DMSO and Et2O; elem. anal.;

Reference yield: 67.0%

: 922171-28-6
Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl

: 536-74-3
phenylacetylene

: 922171-29-7
Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)(C₂C₆H₅)

Guidance literature:: With sodium hydroxide; In methanol; (under N2, Schlenk); ligand and NaOH in MeOH stirred at room temp. for 30 min, Pt-complex added, stirred for 12 h at room temp.; filtered, Et2O diffused into MeCN soln.; elem. anal.;

Reference yield: 63.0%

: 922171-28-6
Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)Cl

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 922171-30-0
Pt(1,3-bis(4'-phenyl-2'-quinolinyl)benzene)(C₂C₆H₄NMe₂-4)

Guidance literature:: With sodium hydroxide; In methanol; (under N2, Schlenk); ligand and NaOH in MeOH stirred at room temp. for 30 min, Pt-complex added, stirred for 12 h at room temp.; filtered, Et2O diffused into MeCN soln.; elem. anal.;