2-butyl-1,4-dihydroxyanthracene-9,10-dione

Base Information

Chemical Name:2-butyl-1,4-dihydroxyanthracene-9,10-dione
CAS No.:23861-69-0
Molecular Formula:C18H16 O4
Molecular Weight:296.3172
Hs Code.:
Mol file:23861-69-0.mol

Synonyms:Anthraquinone,2-butyl-1,4-dihydroxy- (6CI,7CI,8CI); 2-Butyl-1,4-dihydroxy-9,10-anthraquinone;NSC 153373

Suppliers and Price of 2-butyl-1,4-dihydroxyanthracene-9,10-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 2-butyl-1,4-dihydroxyanthracene-9,10-dione

Chemical Property:

Vapor Pressure:4.18E-11mmHg at 25°C
Boiling Point:512°C at 760 mmHg
Flash Point:277.5°C
Density:1.336g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-butyl-1,4-dihydroxyanthracene-9,10-dione

There total 6 articles about 2-butyl-1,4-dihydroxyanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1461-25-2
tetra-n-butyltin(IV)

: 131573-88-1
Trifluoro-methanesulfonic acid 1,4-dihydroxy-9,10-dioxo-9,10-dihydro-anthracen-2-yl ester

: 23861-69-0
1,4-dihydroxy-2-butyl-9,10-anthraquinone

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; lithium chloride; In N,N-dimethyl-formamide; at 90 - 95 ℃; for 2.5h;
DOI:10.1016/S0040-4039(00)97839-0

Reference yield:

: 81-64-1,103220-12-8
1,4-dihydroxy-9,10-anthracenedione

: 123-72-8
butyraldehyde

: 23861-69-0
1,4-dihydroxy-2-butyl-9,10-anthraquinone

Guidance literature:: With sodium dithionite; sodium hydroxide; In methanol; water; at 75 ℃; Inert atmosphere;
DOI:10.1016/j.dyepig.2019.107991

Reference yield:

: 81-54-9
1,2,4-trihydroxy-9,10-anthraquinone

: 23861-69-0
1,4-dihydroxy-2-butyl-9,10-anthraquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 2,6-lutidine, 4-N,N-dimethylaminopyridine / CH₂Cl₂ / 23 °C

2: 74 percent / PdCl₂(PPh₃)2, LiCl / dimethylformamide / 2.5 h / 90 - 95 °C

With 2,6-dimethylpyridine; dmap; bis-triphenylphosphine-palladium(II) chloride; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)97839-0