4-phenyl 1-phenylsulphonyl but-1-ene

Base Information

Chemical Name:4-phenyl 1-phenylsulphonyl but-1-ene
CAS No.:126002-60-6
Molecular Formula:C₁₆H₁₆O₂S
Molecular Weight:272.368
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-phenyl 1-phenylsulphonyl but-1-ene

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Technology Process of 4-phenyl 1-phenylsulphonyl but-1-ene

There total 1 articles about 4-phenyl 1-phenylsulphonyl but-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126002-52-6
4-phenyl-1-phenylsulphonyl-1-(pyridine-2-thiyl)butane

: 87837-53-4,87837-54-5,126002-60-6
4-phenyl 1-phenylsulphonyl but-1-ene

Guidance literature:: With hydrogenchloride; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1) CH₂Cl₂, 4 hr, 20 deg C 2) 100 deg C, 1.5 hr;
DOI:10.1016/S0040-4020(01)96163-0

Reference yield:

: 87837-53-4,87837-54-5,126002-60-6
4-phenyl 1-phenylsulphonyl but-1-ene

: 768-56-9
4-Phenylbut-1-ene

Guidance literature:: With sodium hydroxide; tellurium; sodium tetrahydroborate; Yield given. Multistep reaction; 1) EtOH, reflux 2) -> pH ca. 12, EtOH 3) THF, reflux, ca. 2 hr;
DOI:10.1016/S0040-4020(01)96163-0

Reference yield:

: 1311404-00-8
1-(fluoromethyl)-2-[(S)-p-tolylsulfinyl]benzene

: 87837-53-4,87837-54-5,126002-60-6
4-phenyl 1-phenylsulphonyl but-1-ene

: 1363721-98-5
(2S)-2-((R)-fluoro{2-[(S)-p-tolylsulfinyl]phenyl}methyl)-4-phenylbutyl phenyl sulfone

: 1363721-88-3
(2R)-2-((R)-fluoro{2-[(S)-p-tolylsulfinyl]phenyl}methyl)-4-phenylbutyl phenyl sulfone

Guidance literature:: 1-(fluoromethyl)-2-[(S)-p-tolylsulfinyl]benzene; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere;

4-phenyl 1-phenylsulphonyl but-1-ene; In tetrahydrofuran; hexane; at -78 ℃; for 0.0166667h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo300174k