8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

Base Information

Chemical Name:8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside
CAS No.:90662-46-7
Molecular Formula:C₆₅H₈₄O₂₁
Molecular Weight:1201.37
Hs Code.:

8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

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Chemical Property of 8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

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Technology Process of 8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

There total 13 articles about 8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 90662-43-4
6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-α-D-mannopyranosyl bromide

: 90662-45-6
8-methoxycarbonyloct-1-yl 2,3-O-cyclohexylidene-α-L-rhamnopyranoside

: 90662-46-7
8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) iodide; In chloroform; at 20 ℃; for 96h;

Reference yield:

: 932-92-3
cyclohexyl ethyl ether

: 90662-46-7
8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / p-toluenesulfonic acid / acetonitrile / 0.17 h / 0 - 5 °C

2: 26 percent / mercury(II) iodide, molecular sieves 4 Angstroem / CHCl₃ / 96 h / 20 °C

With 4 A molecular sieve; toluene-4-sulfonic acid; mercury(II) iodide; In chloroform; acetonitrile;

Reference yield:

: 3639-34-7
8-ethoxycarbonyloctanol

: 90662-46-7
8-methoxycarbonyloct-1-yl 4-O-(6-O-acetyl-4-O-allyl-2-O-(6-O-acetyl-2-O-allyl-3,4-di-O-benzoyl-α-D-galactopyranosyl)-3-O-benzyl-β-D-mannopyranosyl)-2,3-O-cyclohexylidene-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 99.5 percent / mercury(II) cyanide, molecular sieves 4 Angstroem / CH₂Cl₂ / 72 h / 20 °C

2: 73.3 g / sodium methoxide / methanol / 2 h / 20 °C

3: 92 percent / p-toluenesulfonic acid / acetonitrile / 0.17 h / 0 - 5 °C

4: 26 percent / mercury(II) iodide, molecular sieves 4 Angstroem / CHCl₃ / 96 h / 20 °C

With 4 A molecular sieve; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury(II) iodide; In methanol; dichloromethane; chloroform; acetonitrile;