C₅₄H₃₆N₆Rh⁽³⁺⁾

Base Information

• Chemical Name: C₅₄H₃₆N₆Rh⁽³⁺⁾
• CAS No.: 81655-93-8
• Molecular Formula: C₅₄H₃₆N₆Rh
• Molecular Weight: 871.826
• Mol file: 81655-93-8.mol

Synonyms:

Chemical Property of C₅₄H₃₆N₆Rh⁽³⁺⁾

Chemical Property:

Purity/Quality:

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Technology Process of C₅₄H₃₆N₆Rh⁽³⁺⁾

There total 1 articles about C₅₄H₃₆N₆Rh⁽³⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rhodium(III) chloride trihydrate + 5-phenyl-1,10-phenanthroline (6153-89-5) → C54H36N6Rh(3+) (81655-93-8)

Guidance literature:

With hydrazine hydrate; In ethanol; water; aq. salt was warmed with ethanolic soln. of ligand until dissolution ofinitial ppt., addition of hydrazine hydrate, refluxed for 24 h; cooling, addition of conc. HClO4, filtration, washing with water, ethanol, ether, drying in vac.;

DOI:10.1021/ja00377a013

upstream raw materials:

5-phenyl-1,10-phenanthroline