carbonylbis(diphenylvinylphosphine)chlororhodium(I)

Base Information

Chemical Name:carbonylbis(diphenylvinylphosphine)chlororhodium(I)
CAS No.:65106-72-1
Molecular Formula:C₂₉H₂₆ClOP₂Rh
Molecular Weight:590.831
Hs Code.:

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Chemical Property of carbonylbis(diphenylvinylphosphine)chlororhodium(I)

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Technology Process of carbonylbis(diphenylvinylphosphine)chlororhodium(I)

There total 1 articles about carbonylbis(diphenylvinylphosphine)chlororhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: di(rhodium)tetracarbonyl dichloride

: 2155-96-6
Diphenylvinylphosphine

: 65106-72-1
carbonylbis(diphenylvinylphosphine)chlororhodium(I)

Guidance literature:: synthesis according to Clark and Harvell, J. Organomet. Chem. 139 (1977)385-401; elem. anal.;

Reference yield: 80.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 65106-72-1
carbonylbis(diphenylvinylphosphine)chlororhodium(I)

: 168136-43-4
carbonylbis(diphenylvinylphosphine)trichlororhodium(III)

Guidance literature:: In chloroform; HCl saturated solvent addn. to soln. of complex, stirring (room temperature, 60 h); solvent evapn. in vacuum, ethanol addn. ppt. filtration off, washing (ethanol), air drying; elem. anal.;

Reference yield: 80.0%

: 65106-72-1
carbonylbis(diphenylvinylphosphine)chlororhodium(I)

: 7782-50-5
chlorine

: 168136-41-2
carbonylbis(diphenyl-1,2-dichloroethylphosphine)-trichlororhodium(III)

Guidance literature:: In chloroform; solvent saturated with chlorine addn. to complex soln., stirring (room temperature, 1 h); soln. partial evapn., ethanol addn., ppt. filtration off, washing (ethanol), air drying; elem. anal.;