prop-2-en-2,3-dihydroxybenzoate

Base Information

• Chemical Name: prop-2-en-2,3-dihydroxybenzoate
• CAS No.: 914370-14-2
• Molecular Formula: C₁₀H₁₀O₄
• Molecular Weight: 194.187
• Mol file: 914370-14-2.mol

Synonyms:

Chemical Property of prop-2-en-2,3-dihydroxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of prop-2-en-2,3-dihydroxybenzoate

There total 2 articles about prop-2-en-2,3-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-Dihydroxybenzoic acid (303-38-8) → prop-2-en-2,3-dihydroxybenzoate (914370-14-2)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / Reflux

2: triethylamine / chloroform / 72 h / Reflux

With thionyl chloride; triethylamine; In chloroform;

DOI:10.1002/chem.201904639

Reference yield:

2,3-hydroxybenzoyl chloride (66168-85-2) + allyl alcohol (107-18-6) → prop-2-en-2,3-dihydroxybenzoate (914370-14-2)

Guidance literature:

With triethylamine; In chloroform; for 72h; Reflux;

DOI:10.1002/chem.201904639

upstream raw materials:

2,3-Dihydroxybenzoic acid

2,3-hydroxybenzoyl chloride

allyl alcohol