diphenylantimony(III) 6-chloro-5-methoxyisatin

Base Information

• Chemical Name: diphenylantimony(III) 6-chloro-5-methoxyisatin
• CAS No.: 152582-24-6
• Molecular Formula: C₂₁H₁₅ClNO₃Sb
• Molecular Weight: 486.558
• Mol file: 152582-24-6.mol

Synonyms:

Chemical Property of diphenylantimony(III) 6-chloro-5-methoxyisatin

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of diphenylantimony(III) 6-chloro-5-methoxyisatin

There total 1 articles about diphenylantimony(III) 6-chloro-5-methoxyisatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

6-chloro-5-methoxy-isatin (85778-01-4) + diphenylantimony(III) chloride (2629-47-2) → diphenylantimony(III) 6-chloro-5-methoxyisatin (152582-24-6)

Guidance literature:

With triethylamine; In methanol; byproducts: NHEt3Cl; stirring of a soln. of Sb-compd. in anhyd. methanol and isatin-compd. in methanol in presence of triethylamine at room temp. (30°C) for 4 h under an anhyd. and O2 free N2 atmosphere; filtn. under N2, removal of NEt3HCl, concn. of filtrate in vacuo, recrystn. from petroleum ether, elem. anal.;

upstream raw materials:

6-chloro-5-methoxy-isatin

diphenylantimony(III) chloride