(Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

Base Information

Chemical Name:(Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride
CAS No.:938452-31-4
Molecular Formula:C₁₀H₉Cl₂NO
Molecular Weight:230.094
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

Chemical Property:

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Technology Process of (Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

There total 5 articles about (Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 938452-28-9
(Z,Z)-O-methyl-β-chlorocinnamohydroximoyl chloride

: 938452-30-3
(E,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

: 938452-31-4
(Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

: 938452-29-0
(E,Z)-O-methyl-β-chlorocinnamohydroximoyl chloride

Guidance literature:: In hexane; for 6h; UV-irradiation;
DOI:10.1071/CH06188

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 938452-31-4
(Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus pentachloride / benzene / 1 h / Heating

2: 3.85 g / triethylamine / CHCl₃ / 4 h / Heating

3: phosphorus pentachloride / 22 h / 20 °C

4: 2 percent / hexane / 6 h / UV-irradiation

With phosphorus pentachloride; triethylamine; In hexane; chloroform; benzene;
DOI:10.1071/CH06188

Reference yield:

: 938452-27-8
3-chloro-N-methoxy-3-phenyl-acrylamide

: 938452-31-4
(Z,E)-O-methyl-β-chlorocinnamohydroximoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentachloride / 22 h / 20 °C

2: 2 percent / hexane / 6 h / UV-irradiation

With phosphorus pentachloride; In hexane;
DOI:10.1071/CH06188