C₂₁H₂₁BrF₂O₆S₂

Base Information

Chemical Name:C₂₁H₂₁BrF₂O₆S₂
CAS No.:1100361-90-7
Molecular Formula:C₂₁H₂₁BrF₂O₆S₂
Molecular Weight:551.427
Hs Code.:

C<sub>21</sub>H<sub>21</sub>BrF<sub>2</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₁H₂₁BrF₂O₆S₂

Chemical Property:

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Technology Process of C₂₁H₂₁BrF₂O₆S₂

There total 8 articles about C₂₁H₂₁BrF₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-53-6
para-bromobenzenethiol

: 1100361-90-7
C₂₁H₂₁BrF₂O₆S₂

Guidance literature:: Multi-step reaction with 12 steps

1: potassium carbonate / tetrahydrofuran

2: lithium aluminium tetrahydride / tetrahydrofuran

3: potassium tert-butylate / tetrahydrofuran

4: Dess-Martin periodane / dichloromethane

5: trimethylsilyl trifluoromethanesulfonate

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane

7: boron trifluoride diethyl etherate / dichloromethane

8: triethylamine / dichloromethane

9: potassium tert-butylate / tetrahydrofuran

10: ozone / dichloromethane

11: triethylamine

12: tetra-(n-butyl)ammonium iodide / tetrahydrofuran

With lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; potassium carbonate; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; 1: |Michael Addition;
DOI:10.1016/j.bmcl.2012.11.047

Reference yield:

: C₁₆H₁₁BrF₂O₂S

: 1100361-90-7
C₂₁H₂₁BrF₂O₆S₂

Guidance literature:: Multi-step reaction with 8 steps

1: trimethylsilyl trifluoromethanesulfonate

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane

3: boron trifluoride diethyl etherate / dichloromethane

4: triethylamine / dichloromethane

5: potassium tert-butylate / tetrahydrofuran

6: ozone / dichloromethane

7: triethylamine

8: tetra-(n-butyl)ammonium iodide / tetrahydrofuran

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047

Reference yield:

: C₂₁H₂₁BrF₂O₅S

: 1100361-90-7
C₂₁H₂₁BrF₂O₆S₂

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane

2: potassium tert-butylate / tetrahydrofuran

3: ozone / dichloromethane

4: triethylamine

5: tetra-(n-butyl)ammonium iodide / tetrahydrofuran

With potassium tert-butylate; tetra-(n-butyl)ammonium iodide; ozone; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047