(C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃

Base Information

Chemical Name:(C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃
CAS No.:502850-30-8
Molecular Formula:C₇H₈*C₇₆H₁₄₀N₄O₁₆Si₈Zn₄
Molecular Weight:1944.35
Hs Code.:

(C<sub>4</sub>H<sub>8</sub>OZnO<sub>2</sub>(OH)Si(C<sub>3</sub>H<sub>7</sub>)2C<sub>6</sub>H<sub>3</sub>NSi(CH<sub>3</sub>)3)4*C<sub>6</sub>H<sub>5</sub>CH<sub>3</sub>

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Chemical Property of (C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃

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Technology Process of (C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃

There total 1 articles about (C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 557-20-0
diethylzinc

: 108-88-3,15644-74-3,16713-13-6
toluene

: 163631-37-6
(2,6-iPr2C6H3)N(SiMe3)Si(OH)3

: 502850-30-8
(C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃

Guidance literature:: In tetrahydrofuran; hexane; toluene; byproducts: C2H6; A soln. of silanol in THF-hexane was added to a soln. of ZnEt2 in toluene-hexane at room temp., the soln. was stirred for 16 h at room temp. (N2); volatiles were removed, the residue was dried for 6 h under vac., washedwith hexane; elem. anal.;
DOI:10.1021/ic020514u

Reference yield: 67.0%

: 502850-30-8
(C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃

: 544-97-8
dimethyl zinc(II)

: 445484-02-6
[Zn₄(ZnMe)4(THF)4(O₃Si(2,6-(CHMe₂)2C₆H₃)N(SiMe₃))4]

Guidance literature:: In tetrahydrofuran; hexane; toluene; byproducts: CH4; a soln. of Zn(CH3)2 in toluene was added to a suspn. of complex in THF-hexane at room temp., stirred for 16 h at room temp. (N2); volatiles were removed, th residue was dried for 6 h under vac., the solid was washed with hexane; recrystd. from toluene at 0°C; elem. anal.;
DOI:10.1021/ic020514u

Reference yield: 45.0%

: 100-22-1
N,N,N',N'-tetramethyl-para-phenylenediamine

: 502850-30-8
(C₄H₈OZnO₂(OH)Si(C₃H₇)2C₆H₃NSi(CH₃)3)4*C₆H₅CH₃

: 917-54-4
methyllithium

: (((CH₃)2N)2C₆H₄ZnLiO₃Si(C₃H₇)2C₆H₃NSi(CH₃)3)4

Guidance literature:: In tetrahydrofuran; diethyl ether; hexane; byproducts: CH4; a soln. of CH3Li in diethyl ether was added to a suspn. of complex in THF-hexane at room temp., stirred for 16 h at room temp., diamine was added, stirred for 4 h (N2); filtered, concd., room temp.;
DOI:10.1021/ic020514u