μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

Base Information

Chemical Name:μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]
CAS No.:20959-77-7
Molecular Formula:C₁₂H₁₀Fe₂N₄O₄S₂
Molecular Weight:450.062
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

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Technology Process of μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

There total 4 articles about μ2-S-[bis(benzenethiolato)tetranitrosyldiiron] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: Sodium thiosulfate pentahydrate

: Na₂[Fe₂(thiosulfato)2(NO)4]*4H₂O

: 108-98-5
thiophenol

: 20959-77-7,1262207-74-8,1031443-01-2
μ2-S-[bis(benzenethiolato)tetranitrosyldiiron]

Guidance literature:: With NaOH; In water; H2O satd. with Ar for 30 min and added to a mixt. of Na2S2O3*5H2O, Fe complex, NaOH, and C6H5SH; stirred at ca 20°C for 2 h; extd. (CH2Cl2), concd., filtered, crystd. on air for hours, dried in air; elem. anal.;
DOI:10.1007/s11172-010-0215-z

Reference yield:

: 16921-91-8
nitrosyl hexafluorophosphate

: 119435-51-7
{PPN}{PhSFe(CO)4}

: 15634-63-6
{PhSFe(CO)3}2

: 20959-77-7
{PhSFe(NO)2}2

Guidance literature:: In tetrahydrofuran; mixt. of educts (molar ratio 1:1) in THF, -78°C, 20 min stirred, warmed to room temp.;
DOI:10.1021/ja00192a016