2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline

Base Information

Chemical Name:2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline
CAS No.:1357392-28-9
Molecular Formula:C₂₃H₁₄N₄O
Molecular Weight:362.39
Hs Code.:

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Chemical Property of 2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline

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Technology Process of 2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline

There total 1 articles about 2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 13803-39-9
5-phenylfuran-2-carbaldehyde

: 27318-90-7
1,10-phenanthroline-5,6-dione

: 1357392-28-9
2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline

Guidance literature:: 5-phenylfuran-2-carbaldehyde; 1,10-phenanthroline-5,6-dione; With ammonium acetate; acetic acid; for 5h; Reflux;

With ammonium hydroxide; at 20 ℃;
DOI:10.1016/j.ica.2011.07.020

Reference yield: 96.0%

: ammonium hexafluorophosphate

: cis-dichloro(2,2′-bipyridine)ruthenium(II)chloride

: 1357392-28-9
2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline

: [Ru(bpy)2(2-(5'-phenylfuran-2'-yl)-1H-imidazo[4,5-f][1,10]phenanthroline)](PF₆)2

Guidance literature:: In ethylene glycol; other Radiation; Ru complex and phenanthroline deriv. dissolved in ethanediol; heated in microwave oven (450 W, 30 s); allowed to cool, procedure repeated 3 times more; solvent removed by distillation; residue dissolved in H2O, aq. NH4PF6 added; ppt. filtered through frit, washed with water and Et2O; dried undervac.; elem. anal.;