chloro-((diphenylphosphino)acetate-κ2P,O)(η5-pentamethylcyclopentadienyl)rhodium(III)-trimethylstannyl chloride

Base Information

• Chemical Name: chloro-((diphenylphosphino)acetate-κ2P,O)(η5-pentamethylcyclopentadienyl)rhodium(III)-trimethylstannyl chloride
• CAS No.: 800377-07-5
• Molecular Formula: C₂₇H₃₆Cl₂O₂PRhSn
• Molecular Weight: 716.077
• Mol file: 800377-07-5.mol

Synonyms:

Chemical Property of chloro-((diphenylphosphino)acetate-κ2P,O)(η5-pentamethylcyclopentadienyl)rhodium(III)-trimethylstannyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chloro-((diphenylphosphino)acetate-κ2P,O)(η5-pentamethylcyclopentadienyl)rhodium(III)-trimethylstannyl chloride

There total 1 articles about chloro-((diphenylphosphino)acetate-κ2P,O)(η5-pentamethylcyclopentadienyl)rhodium(III)-trimethylstannyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer + trimethylstannyl (diphenylphosphino)acetate (800377-04-2) → chloro-((diphenylphosphino)acetate-κ2P,O)(η5-pentamethylcyclopentadienyl)rhodium(III)-trimethylstannyl chloride (800377-07-5)

Guidance literature:

In dichloromethane; under Ar; Rh complex and Sn compd. dissolved in CH2Cl2; stirred overnight; layered with hexane; crystd. by liq. phase diffusion over several d; elem. anal.;

DOI:10.1016/j.jorganchem.2004.07.060

upstream raw materials:

trimethylstannyl (diphenylphosphino)acetate