trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

Base Information

Chemical Name:trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']
CAS No.:133323-50-9
Molecular Formula:C₃₆H₃₆MoO₇P₂
Molecular Weight:738.565
Hs Code.:

trans-Mo(CO)4[Ph<sub>2</sub>P(CH<sub>2</sub>CH<sub>2</sub>O)3CH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>-P,P']

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

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Technology Process of trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

There total 2 articles about trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P'] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 12146-37-1,124717-04-0
cis-{Mo(CO)4(bicyclo{2.2.1}-hepta-2,5-diene)}

: 98583-60-9
2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

: 133323-50-9,357397-00-3
cis-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

Guidance literature:: In dichloromethane; (N2), solutions of Mo-compd. and ligand in CH2Cl2 were added dropwise to CH2Cl2 over a period of 5 h,stirred for 18 h; evaporated, treated with silica gel before filtered, washed with dichloromethane-hexanes mixture, filtrate evaporated to dryness,;

Reference yield: 24.0%

: 133323-50-9,357397-00-3
cis-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

: 133323-50-9,357397-00-3
trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); THF was poured into reactor, purged for 10 min with N2, Mo-complex was added, irradiated with 350 W mercury lamp for 20 min; evapd. to dryness, dissolved in CH2Cl2, filtered through silica gel, concd., TLC with ethyl acetate/hexane, eluted with MeOH, evapd. to dryness,dried for 2 h under high vac.; elem. anal.;
DOI:10.1016/S0020-1693(01)00350-4

Reference yield: 24.0%

: 133323-50-9,357397-00-3
cis-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

: 133323-50-9,357397-00-3
trans-Mo(CO)4[Ph₂P(CH₂CH₂O)3CH₂CH₂PPh₂-P,P']

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); THF was poured into reactor, purged for 10 min with N2, Mo-complex was added, irradiated with 350 W mercury lamp for 20 min; evapd. to dryness, dissolved in CH2Cl2, filtered through silica gel, concd., TLC with ethyl acetate/hexane, eluted with MeOH, evapd. to dryness,dried for 2 h under high vac.; elem. anal.;
DOI:10.1016/S0020-1693(01)00350-4