2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

Base Information

Chemical Name:2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether
CAS No.:98583-60-9
Molecular Formula:C₃₂H₃₆O₃P₂
Molecular Weight:530.584
Hs Code.:

Synonyms:2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

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Chemical Property of 2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

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Technology Process of 2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

There total 1 articles about 2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 764-99-8,50856-26-3
diethylene glycol divinyl ether

: 829-85-6
diphenylphosphane

: 98583-60-9
2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 65 ℃; for 48h; chemoselective reaction; Inert atmosphere;
DOI:10.1055/s-0032-1316764

Reference yield: 97.0%

: 98583-60-9
2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

: 74-88-4
methyl iodide

: C₃₄H₄₂O₃P₂⁽²⁺⁾*2I^(1-)

Guidance literature:: In dichloromethane; at 23 - 25 ℃; for 1h; Inert atmosphere;
DOI:10.1055/s-0032-1316764

Reference yield: 89.0%

: 33677-56-4
Pt(dba)2

: 98583-60-9
2-{2-[2-(diphenylphosphino)ethoxy]ethoxy}ethyl 2-(diphenylphosphino)ethyl ether

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 740846-61-1
platinum(O)(η2-C60)[Ph2PCH2(CH2OCH2)3CH2PPh2]

Guidance literature:: In toluene; (N2) Pd:C60:L=1:1:1, C60 in toluene treated with Pd complex , stirred atroom temp. for 30 min, treated with ligand, stirred for 0.5 h; layered with hexane, standed overnight, filtered, washed (toluene), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200300513