N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide

Base Information

Chemical Name:N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide
CAS No.:1210811-82-7
Molecular Formula:C₂₃H₁₉FeNO
Molecular Weight:381.257
Hs Code.:

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Chemical Property of N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide

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Technology Process of N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide

There total 2 articles about N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1210811-81-6
4'-ferrocenyl[1,1' ]biphenyl-4-amine

: 2258-42-6
formyl acetic anhydride

: 1210811-82-7
N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide

Guidance literature:: In tetrahydrofuran; Fc deriv. in THF added with stirring to cold (-20°C) THF soln. ofacetic formic anhydride; stirred for 10 min; solvent removed in vacuo; elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.043

Reference yield: 70.0%

: tris(4-ferrocenylphenyl)boroxine

: 2617-78-9
N-(4-bromophenyl)formamide

: 1210811-82-7
N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide

Guidance literature:: With K₂CO₃; In water; boroxine, 4-bromoformanilide reacted in DMF/water in presence of Pd(PPh3)4; chromy. on silica gel (eluent CHCl3/ether);
DOI:10.1016/j.jorganchem.2009.09.043

Reference yield: 81.0%

: 1210811-82-7
N-(4'-ferrocenyl[1,1']biphenyl-4-yl)formamide

: 503-38-8
trichloromethyl chloroformate

: 1210811-95-2
(ferrocenyl)(C₆H₄)2(isocyanide)

Guidance literature:: With triethylamine; In chloroform; diphosgene soln. in CHCl3 added with stirring to refluxing suspn. of Fc deriv. in mixt. of Et3N and CHCl3; react. mixt. stirred under reflux for20 min, cooled to ambient temp.; washed with 10% soln. of Na2CO3; org. layer separated, dried over Na2SO4; solvent removed on rotary evaporator; chromy. on silica gel (eluent CHCl3/petroleum ether); elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.043