E-β-styrylgermatrane

Base Information

Chemical Name:E-β-styrylgermatrane
CAS No.:490020-65-0
Molecular Formula:C₁₄H₁₉GeNO₃
Molecular Weight:321.9
Hs Code.:

Synonyms:

Suppliers and Price of E-β-styrylgermatrane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E-β-styrylgermatrane

Chemical Property:

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Technology Process of E-β-styrylgermatrane

There total 5 articles about E-β-styrylgermatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67453-19-4
germatrane

: 536-74-3
phenylacetylene

: [C₆H₅C(CH₂)Ge(OCH₂CH₂)3N]

: 312958-73-9,490020-65-0
Z-β-styrylgermatrane

: 312958-73-9,490020-65-0
E-β-styrylgermatrane

Guidance literature:: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In toluene; (N2); standard Schlenk technique; toluene was added to mixt. of Ge compd. and Rh catalyst; arylacetylene was added; soln. was refluxed for 12 h; soln. passed through pad of Celite; residue washed with CH2Cl2; solvent from filtrate and washings removed (vac.); residue dissolved in CH3CN; chromd. (reversed-phase silica gel, CH3CN);
DOI:10.1021/om020714d

Reference yield: 80.0%

: 67453-19-4
germatrane

: 536-74-3
phenylacetylene

: [C₆H₅C(CH₂)Ge(OCH₂CH₂)3N]

: 312958-73-9,490020-65-0
Z-β-styrylgermatrane

: 312958-73-9,490020-65-0
E-β-styrylgermatrane

Guidance literature:: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In toluene; (N2); standard Schlenk technique; toluene was added to mixt. of Ge compd. and Rh catalyst; arylacetylene was added; soln. was refluxed for 12 h; soln. passed through pad of Celite; residue washed with CH2Cl2; solvent from filtrate and washings removed (vac.); residue dissolved in CH3CN; chromd. (reversed-phase silica gel, CH3CN);
DOI:10.1021/om020714d

Reference yield: 71.0%

: 67453-19-4
germatrane

: 536-74-3
phenylacetylene

: 312958-73-9,490020-65-0
E-β-styrylgermatrane

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; (N2); standard Schlenk technique; toluene was added via syringe to mixt.of Ge compd. and Pd catalyst; arylacetylene was added; soln. was reflux ed for 17.5 h; mixt. passed through pad of Celite; solvent removed (vac.); ether added;
DOI:10.1021/om020714d