C₅₆H₄₀N₄O₆S₂

Base Information

Chemical Name:C₅₆H₄₀N₄O₆S₂
CAS No.:1351663-39-2
Molecular Formula:C₅₆H₄₀N₄O₆S₂
Molecular Weight:929.089
Hs Code.:

C<sub>56</sub>H<sub>40</sub>N<sub>4</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₅₆H₄₀N₄O₆S₂

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Technology Process of C₅₆H₄₀N₄O₆S₂

There total 6 articles about C₅₆H₄₀N₄O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1351663-37-0
p,p'-bis{N-[4-(5-formyl-thien-2-yl)phenyl]-N-(4-methoxyphenyl)-amino}stilbene

: 372-09-8
cyanoacetic acid

: 1351663-39-2
C₅₆H₄₀N₄O₆S₂

Guidance literature:: With piperidine; In ethanol; at 100 ℃; for 1h; Microwave irradiation;
DOI:10.1002/ejoc.201100821

Reference yield:

: 1351663-31-4
4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzaldehyde

: 1351663-39-2
C₅₆H₄₀N₄O₆S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / ethanol / 0 - 20 °C

2.1: iodine / 0 - 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / Cooling with ice

3.2: 24 h / 0 - 20 °C

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / methanol; toluene / 0.17 h / 70 °C / Microwave irradiation

5.1: piperidine / ethanol / 1 h / 100 °C / Microwave irradiation

With piperidine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; potassium tert-butylate; iodine; potassium carbonate; In tetrahydrofuran; methanol; ethanol; toluene; 3.1: Horner-Wittig condensation / 3.2: Horner-Wittig condensation / 4.1: Suzuki coupling / 5.1: Knoevenagel condensation;
DOI:10.1002/ejoc.201100821

Reference yield:

: 87755-82-6
4-[N-phenyl-N-(4-methoxyphenyl)amino]benzaldehyde

: 1351663-39-2
C₅₆H₄₀N₄O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / -5 - 0 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 0 - 20 °C

3.1: iodine / 0 - 20 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / Cooling with ice

4.2: 24 h / 0 - 20 °C

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / methanol; toluene / 0.17 h / 70 °C / Microwave irradiation

6.1: piperidine / ethanol / 1 h / 100 °C / Microwave irradiation

With piperidine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; N-Bromosuccinimide; potassium tert-butylate; iodine; potassium carbonate; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene; 4.1: Horner-Wittig condensation / 4.2: Horner-Wittig condensation / 5.1: Suzuki coupling / 6.1: Knoevenagel condensation;
DOI:10.1002/ejoc.201100821