methyl o-(dimethylstibino)phenyl telluride

Base Information

Chemical Name:methyl o-(dimethylstibino)phenyl telluride
CAS No.:120058-46-0
Molecular Formula:C₉H₁₃SbTe
Molecular Weight:370.552
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl o-(dimethylstibino)phenyl telluride

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Technology Process of methyl o-(dimethylstibino)phenyl telluride

There total 1 articles about methyl o-(dimethylstibino)phenyl telluride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 34666-93-8
(o-bromophenyl)dimethylstibine

: 20334-43-4
dimethyl ditelluride

: 120058-46-0
methyl o-(dimethylstibino)phenyl telluride

Guidance literature:: With n-butyllithium; In diethyl ether; all manipulations under dry N2; adding n-BuLi in Et2O to a soln. of (o-bromophenyl)dimethylstibine in dry Et2O (-63°C), stirring (3 h, -63°C), warming to room temp., adding dropwise Me2Te2, standing (2 h), adding H2O; extg. (Et2O), drying extract (over MgSO4, 16 h), removing solvent (vacuum), fractionating residue, chromy. of fraction boiling at 144°C (0.3 Torr) (silica gel, exclusion of air, petroleum ether, 40 - 60°C);
DOI:10.1021/om00107a028