(o-bromophenyl)dimethylstibine

Base Information

Chemical Name:(o-bromophenyl)dimethylstibine
CAS No.:34666-93-8
Molecular Formula:C₈H₁₀BrSb
Molecular Weight:307.821
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (o-bromophenyl)dimethylstibine

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Technology Process of (o-bromophenyl)dimethylstibine

There total 1 articles about (o-bromophenyl)dimethylstibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 917-64-6
methyl magnesium iodide

: 34666-92-7
2-BrC₆H₅SbCl₂

: 34666-93-8
(o-bromophenyl)dimethylstibine

Guidance literature:: In diethyl ether;
DOI:10.1021/ic50106a009

Reference yield: 70.0%

: 14104-20-2
silver tetrafluoroborate

: 34666-93-8
(o-bromophenyl)dimethylstibine

: 176769-77-0
[Ag(SbMe₂(o-C₆H₄Br))4]BF₄

Guidance literature:: In acetone; N2-atmosphere; addn. of AgBF4 to stoich. amts. stibine (ice-cold soln., in dark), stirring for 1 h; filtration, solvent removal (vac.), washing (pentane), drying (vac.); elem. anal.;

Reference yield: 29.0%

: 34666-93-8
(o-bromophenyl)dimethylstibine

: 21743-25-9
lithium dimethylphosphide

: 72565-25-4
(o-dimethylphosphinophenyl)dimethylstibine

: 17585-86-3
dimethyl(phenyl)stibine

Guidance literature:: In tetrahydrofuran; N2-atmosphere; dropwise addn. of 1 equiv. LiPMe2 to BrC6H4SbMe2 (0°C), stirring (room temp., 3 h), refluxing (1 h); addn. of H2O, sepn. of org. layer, drying, distn. off of SbMe2Ph;
DOI:10.1039/DT9790001718