sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾

Base Information

Chemical Name:sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾
CAS No.:141327-10-8
Molecular Formula:C₃₆H₃₀OP₂PdS
Molecular Weight:679.067
Hs Code.:

sulfurmonoxide{bis(triphenylphosphane)}palladium<sup>(0)</sup>

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Chemical Property of sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾

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Technology Process of sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾

There total 1 articles about sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 7117-41-1
thiirane 1-oxide

: 141327-10-8
sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾

Guidance literature:: In toluene; addn. of C2H4SO (1 mmol) to Pd(PPh3)4 (0.199 mmol) in toluene, stirring; pptn. after 2h; addn. of n-hexane, pptn.; washing (n-hexane), drying (vac.); elem. anal.;

Reference yield: 47.0%

: 141327-10-8
sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

: 141327-09-5
thiosulfato-O,S{bis(triphenylphosphane)}palladium(II)

Guidance literature:: In toluene; satn. of SO2 with toluene; addn. to (PPh3)2PdSO, stirring, SO2 atmosphere; stirring brown suspn. 12 h; addn. of n-hexane to soln., pptn.; drying (vac.); elem. anal.;

Reference yield: 25.0%

: 141327-10-8
sulfurmonoxide{bis(triphenylphosphane)}palladium⁽⁰⁾

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: [(Pd(PPh₃)2)n]

: 2,5-dihydro-3,4-dimethyl-thiophene 1-oxide

Guidance literature:: In tetrahydrofuran; dissolvin Pd complex in THF; addn. of butadiene; refluxing, 6h; addn. of petroleum ether, pptn.; evapn. of filtrate; spectroscopic detn.;