(1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate

Base Information Edit

Chemical Name:(1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate
CAS No.:33116-78-8
Molecular Formula:C₁₇H₂₄O₄S
Molecular Weight:324.441
Hs Code.:
Mol file:33116-78-8.mol

Synonyms:

Suppliers and Price of (1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate

There total 3 articles about (1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 22556-08-7
trans-3,4-caranediol

: 98-59-9
p-toluenesulfonyl chloride

: 33116-78-8,39815-45-7,52153-56-7,57129-21-2,77448-79-4
(1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate

Guidance literature:: With pyridine; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.tetasy.2009.12.001

Reference yield:

: 498-15-7,19079-29-9
(+)-Δ³-carene

: 33116-78-8,39815-45-7,52153-56-7,57129-21-2,77448-79-4
(1S,3R)-(+)-3-hydroxy-4-isocaranyl tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / silver acetate, iodine / acetic acid; H₂O / 4 h / Heating

2: 8 N Jones reagent / 0.5 h

3: pyridine

With pyridine; jones reagent; iodine; silver(I) acetate; In water; acetic acid;