Technology Process of C26H38O4
There total 5 articles about C26H38O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,10-bis(2,4-bis(ethoxycarbonyl)phenyl)decane;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
Inert atmosphere;
With
hydrogenchloride;
In
tetrahydrofuran; ethanol; water; ethyl acetate;
Inert atmosphere;
DOI:10.1021/jo201013q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon; hydrogen / ethanol / 18 h / 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
2.2: Inert atmosphere
With
lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; ethanol;
DOI:10.1021/jo201013q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 18 h / 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; ethanol;
DOI:10.1021/jo201013q