4‐(2‐ferrocenylvinyl)benzaldehyde

Base Information

Chemical Name:4‐(2‐ferrocenylvinyl)benzaldehyde
CAS No.:123931-08-8
Molecular Formula:C₁₉H₁₆FeO
Molecular Weight:316.182
Hs Code.:

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Chemical Property of 4‐(2‐ferrocenylvinyl)benzaldehyde

Chemical Property:

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Technology Process of 4‐(2‐ferrocenylvinyl)benzaldehyde

There total 3 articles about 4‐(2‐ferrocenylvinyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 877307-36-3,877459-62-6
(C₅H₅)Fe(C₅H₄CHCHC₆H₄C₄H₅(CH₃)2O₂)

: 76-05-1
trifluoroacetic acid

: 123931-08-8,72022-45-8,98243-45-9
4‐(2‐ferrocenylvinyl)benzaldehyde

Guidance literature:: With water; In dichloromethane; a 1:1 mixt. of CF3CO2H/H2O was added to a degassed soln. of complex in CH2Cl2 under Ar, the mixt. was stirred at room temp. for 5 h under Ar; washed with H2O, (until pH was neat neutrality), dried over MgSO4, filtered, evapd. to dryness, column chromy. (silica gel, CH2Cl2/hexane 1:1); elem. anal.;
DOI:10.1039/b711030h

Reference yield: 75.0%

: 223134-54-1
ferrocene methyl triphenylphosphine hydrobromate

: 623-27-8
terephthalaldehyde,

: 123931-08-8,72022-45-8,98243-45-9
4‐(2‐ferrocenylvinyl)benzaldehyde

Guidance literature:: With potassium t-butoxide; In tetrahydrofuran; refluxing Fe-complex with 4 equiv. of aldehyde for 4 h; addn. of H2O, extn. into Et2O, washing (brine), drying (MgSO4), evapn., chromy. (SiO2, CH2Cl2/hexane=1:4);
DOI:10.1016/S0022-328X(98)01009-2

Reference yield:

: 1271-51-8
vinyl ferrocene

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 123931-08-8,72022-45-8,98243-45-9
4‐(2‐ferrocenylvinyl)benzaldehyde

Guidance literature:: With palladium diacetate; triethylamine; Tri(p-tolyl)phosphine; In acetonitrile; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c7dt01952a