1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate

Base Information

Chemical Name:1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate
CAS No.:1263140-38-0
Molecular Formula:C₂₈H₁₂Cl₇F₃O₄
Molecular Weight:717.567
Hs Code.:

Synonyms:

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Chemical Property of 1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate

Chemical Property:

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Technology Process of 1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate

There total 8 articles about 1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447649-19-5
C₁₆H₈Cl₃F₃O₂

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 1263140-38-0
1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate

Guidance literature:: In dichloromethane;

Reference yield:

: 56911-48-9
diethyl (3-bromophenyl)malonate

: 1263140-38-0
1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane; water / 0.5 h / 80 °C

2.1: sodium hydroxide; water / 0.33 h / 50 °C

2.2: 10 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / Inert atmosphere

4.1: dichloromethane

With oxalyl dichloride; water; sodium carbonate; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: (2-chloro-4-(trifluoromethyl)phenyl)boronic acid

: 1263140-38-0
1,3-bis(2,4,6-trichlorophenyl) 2-[2'-chloro-4'-(trifluoromethyl)[1,1'-biphenyl]-3-yl]propanedioate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane; water / 0.5 h / 80 °C

2.1: sodium hydride / mineral oil

3.1: sodium hydroxide; water / 0.33 h / 50 °C

3.2: 10 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / Inert atmosphere

5.1: dichloromethane

With oxalyl dichloride; water; sodium hydride; sodium carbonate; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; water; mineral oil;