(FcCC)2CHPhOH

Base Information

Chemical Name:(FcCC)2CHPhOH
CAS No.:906648-37-1
Molecular Formula:C₃₁H₂₄Fe₂O
Molecular Weight:524.225
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (FcCC)2CHPhOH

Chemical Property:

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Technology Process of (FcCC)2CHPhOH

There total 1 articles about (FcCC)2CHPhOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 1271-47-2
ferroceneacetylene

: 906648-37-1
(FcCC)2CHPhOH

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; addn. of soln. of BuLi in hexane to soln. of acetylene deriv. in THF at -78°C, stirring for 30 min, addn. of methyl benzoate, keeping at -78°C for 1 h, warming to room temp. over 1 h; pouring into ice, evapn., extn. (ether), washing with H2O, saturd. aqueous NaCl, drying by K2CO3, filtration, evapn., passing through SiO2, eluting impurities with petroleum ether/CH3COOEt (100:1), eluting product with CH3COOEt, recrystn. CH2Cl2/C5H12);
DOI:10.1016/j.jorganchem.2006.04.002

Reference yield:

: 906648-37-1
(FcCC)2CHPhOH

: 906648-57-5
((FcCC)2CPh)(trifluoroacetate)

Guidance literature:: With HBF₄ or HPF₆ or Ph₃CBF₄; treating iron compd. with ethereal HBF4 or aqueous HPF6 or Ph3CBF4; NMR;
DOI:10.1016/j.jorganchem.2006.04.002

Reference yield:

: 906648-37-1
(FcCC)2CHPhOH

: 76-05-1
trifluoroacetic acid

: 906648-57-5
((FcCC)2CPh)(trifluoroacetate)

Guidance literature:: In dichloromethane; addn. of trifluoroacetic acid to soln. of iron compd. in dry CH2Cl2; detected by UV-Vis-NIR;
DOI:10.1016/j.jorganchem.2006.04.002