Technology Process of C30H33ClN6O17P2
There total 5 articles about C30H33ClN6O17P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
2: N,N-dimethyl-formamide / 50 °C / pH 8.1 / aq. phosphate buffer
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201100940
- Guidance literature:
-
Multi-step reaction with 3 steps
1: inorganic pyrophosphatase; L-fucokinase pyrophosphorylase; tris hydrochloride; manganese(ll) chloride; ATP / 12 h / 37 °C / Enzymatic reaction
2: palladium 10% on activated carbon; hydrogen / water / 0.25 h
3: N,N-dimethyl-formamide / 50 °C / pH 8.1 / aq. phosphate buffer
With
inorganic pyrophosphatase; palladium 10% on activated carbon; L-fucokinase pyrophosphorylase; hydrogen; tris hydrochloride; manganese(ll) chloride; ATP;
In
water; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201100940
- Guidance literature:
-
Multi-step reaction with 3 steps
1: inorganic pyrophosphatase; L-fucokinase pyrophosphorylase; tris hydrochloride; manganese(ll) chloride; ATP / 12 h / 37 °C / Enzymatic reaction
2: palladium 10% on activated carbon; hydrogen / water / 0.25 h
3: N,N-dimethyl-formamide / 50 °C / pH 8.1 / aq. phosphate buffer
With
inorganic pyrophosphatase; palladium 10% on activated carbon; L-fucokinase pyrophosphorylase; hydrogen; tris hydrochloride; manganese(ll) chloride; ATP;
In
water; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201100940