Technology Process of C29H26N2O7S
There total 5 articles about C29H26N2O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: piperidine; sulfur / ethanol / 4 h / 50 °C
2: chloranil / 1,4-dioxane / 5 h / 90 °C
3: hydrogenchloride / butan-1-ol / 2 h / Reflux
With
piperidine; hydrogenchloride; chloranil; sulfur;
In
1,4-dioxane; ethanol; butan-1-ol;
1: Gewald reaction;
DOI:10.1016/j.tetlet.2010.12.081
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C
2: piperidine; sulfur / ethanol / 4 h / 50 °C
3: chloranil / 1,4-dioxane / 5 h / 90 °C
4: hydrogenchloride / butan-1-ol / 2 h / Reflux
With
piperidine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; chloranil; sulfur;
In
1,4-dioxane; ethanol; ethyl acetate; butan-1-ol;
2: Gewald reaction;
DOI:10.1016/j.tetlet.2010.12.081
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C
3: piperidine; sulfur / ethanol / 4 h / 50 °C
4: chloranil / 1,4-dioxane / 5 h / 90 °C
5: hydrogenchloride / butan-1-ol / 2 h / Reflux
With
piperidine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; chloranil; sulfur; trifluoroacetic acid;
In
1,4-dioxane; ethanol; dichloromethane; ethyl acetate; butan-1-ol;
3: Gewald reaction;
DOI:10.1016/j.tetlet.2010.12.081