C₄₃H₆₅BF₂N₈O₁₂

Base Information

• Chemical Name: C₄₃H₆₅BF₂N₈O₁₂
• CAS No.: 1425860-85-0
• Molecular Formula: C₄₃H₆₅BF₂N₈O₁₂
• Molecular Weight: 934.843
• Mol file: 1425860-85-0.mol

Synonyms:

Chemical Property of C₄₃H₆₅BF₂N₈O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₃H₆₅BF₂N₈O₁₂

There total 4 articles about C₄₃H₆₅BF₂N₈O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

C35H45BF2N4O8 (1425860-89-4) + 2,2'-iminobis[ethanol] (111-42-2) → C43H65BF2N8O12 (1425860-85-0)

Guidance literature:

In acetonitrile; for 24h; Inert atmosphere; Reflux;

DOI:10.1039/c2dt32531d

Reference yield:

1,2-diamino-benzene (95-54-5) → C43H65BF2N8O12 (1425860-85-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 8 h / Reflux

2.1: trichlorophosphate / 2 h

3.1: trifluoroacetic acid / dichloromethane / 10 h / 20 °C / Inert atmosphere

3.2: 4 h / 20 °C / Inert atmosphere

3.3: 2 h / 20 °C / Inert atmosphere

4.1: acetonitrile / 24 h / Inert atmosphere; Reflux

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium iodide; trichlorophosphate; In dichloromethane; acetonitrile; 2.1: |Vilsmeier-Haack Formylation;

DOI:10.1039/c2dt32531d

Reference yield:

tetraethyl 2,2',2'',2'''-(1,2-phenylenebis(azanetriyl))tetraacetate (897054-41-0) → C43H65BF2N8O12 (1425860-85-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: trichlorophosphate / 2 h

2.1: trifluoroacetic acid / dichloromethane / 10 h / 20 °C / Inert atmosphere

2.2: 4 h / 20 °C / Inert atmosphere

2.3: 2 h / 20 °C / Inert atmosphere

3.1: acetonitrile / 24 h / Inert atmosphere; Reflux

With trifluoroacetic acid; trichlorophosphate; In dichloromethane; acetonitrile; 1.1: |Vilsmeier-Haack Formylation;

DOI:10.1039/c2dt32531d

upstream raw materials:

C₃₅H₄₅BF₂N₄O₈

2,2'-iminobis[ethanol]

1,2-diamino-benzene

tetraethyl 2,2',2'',2'''-(1,2-phenylenebis(azanetriyl))tetraacetate