C₁₄H₁₁⁽²⁾HOS

Base Information

Chemical Name:C₁₄H₁₁⁽²⁾HOS
CAS No.:1440664-91-4
Molecular Formula:C₁₄H₁₂OS
Molecular Weight:229.307
Hs Code.:

C<sub>14</sub>H<sub>11</sub><sup>(2)</sup>HOS

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Suppliers and Price of C₁₄H₁₁⁽²⁾HOS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₁⁽²⁾HOS

Chemical Property:

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Technology Process of C₁₄H₁₁⁽²⁾HOS

There total 2 articles about C₁₄H₁₁⁽²⁾HOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104977-33-5
trans-β-(methyl-d3)styrene

: 1440664-91-4
C₁₄H₁₁⁽²⁾HOS

Guidance literature:: Multi-step reaction with 3 steps

1: 5%-palladium/activated carbon; hydrogen / 24 h / 20 °C / Inert atmosphere

2: iron(III) chloride; potassium permanganate / acetone / 20 h / -78 - 20 °C / Inert atmosphere

3: palladium diacetate; tricyclohexylphosphine; lithium acetate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; silver (II) carbonate / 1,2-dimethoxyethane / 24 h / 100 °C / Schlenk technique; Inert atmosphere

With iron(III) chloride; silver (II) carbonate; potassium permanganate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 5%-palladium/activated carbon; lithium acetate; hydrogen; palladium diacetate; tricyclohexylphosphine; In 1,2-dimethoxyethane; acetone;
DOI:10.1002/anie.201208627

Reference yield:

: 536-74-3
phenylacetylene

: 1440664-91-4
C₁₄H₁₁⁽²⁾HOS

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 - 0 °C / Inert atmosphere

1.2: 2 h / -20 - 20 °C

2.1: 5%-palladium/activated carbon; hydrogen / 24 h / 20 °C / Inert atmosphere

3.1: iron(III) chloride; potassium permanganate / acetone / 20 h / -78 - 20 °C / Inert atmosphere

4.1: palladium diacetate; tricyclohexylphosphine; lithium acetate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; silver (II) carbonate / 1,2-dimethoxyethane / 24 h / 100 °C / Schlenk technique; Inert atmosphere

With iron(III) chloride; silver (II) carbonate; potassium permanganate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 5%-palladium/activated carbon; lithium acetate; hydrogen; palladium diacetate; tricyclohexylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; acetone;
DOI:10.1002/anie.201208627