C₆₀H₇₈Cl₂Cu₂P₂

Base Information

• Chemical Name: C₆₀H₇₈Cl₂Cu₂P₂
• CAS No.: 1447322-44-2
• Molecular Formula: C₆₀H₇₈Cl₂Cu₂P₂
• Molecular Weight: 1059.22
• Mol file: 1447322-44-2.mol

Synonyms:

Chemical Property of C₆₀H₇₈Cl₂Cu₂P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₇₈Cl₂Cu₂P₂

There total 2 articles about C₆₀H₇₈Cl₂Cu₂P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,6-diisopropylphenyl)magnesium bromide → C60H78Cl2Cu2P2 (1447322-44-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / -70 - 20 °C / Inert atmosphere

2: 5,5-dimethyl-1,3-cyclohexadiene / 20 h / Inert atmosphere; Reflux

In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene;

DOI:10.1021/ja403555d

Reference yield:

C12H17Cu + Dichlorophenylphosphine (644-97-3) → C36H44Cl4Cu2P2 + C60H78Cl2Cu2P2 (1447322-44-2)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; for 20h; Inert atmosphere; Reflux;

DOI:10.1021/ja403555d

Reference yield:

C60H78Cl2Cu2P2 (1447322-44-2) → oxo bis(2,6-diisopropylphenyl)phenylphosphane (1447322-52-2)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonia / 5,5-dimethyl-1,3-cyclohexadiene; water / Inert atmosphere

2: dihydrogen peroxide / acetone / Inert atmosphere; Heating

With ammonia; dihydrogen peroxide; In 5,5-dimethyl-1,3-cyclohexadiene; water; acetone;

DOI:10.1021/ja403555d

upstream raw materials:

Dichlorophenylphosphine

Downstream raw materials:

oxo bis(2,6-diisopropylphenyl)phenylphosphane

sulfido bis(2,6-diisopropylphenyl)phenylphosphane

bis(2,6-diisopropylphenyl)phenylphosphine selenide

C₃₀H₃₉P