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MeN(CH2-2-C6H4SbMe2)2

Base Information
  • Chemical Name:MeN(CH2-2-C6H4SbMe2)2
  • CAS No.:1195345-85-7
  • Molecular Formula:C19H27NSb2
  • Molecular Weight:512.93
  • Hs Code.:
MeN(CH<sub>2</sub>-2-C<sub>6</sub>H<sub>4</sub>SbMe<sub>2</sub>)2

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Chemical Property of MeN(CH2-2-C6H4SbMe2)2
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Technology Process of MeN(CH2-2-C6H4SbMe2)2

There total 1 articles about MeN(CH2-2-C6H4SbMe2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With butyllithium; H2O; In diethyl ether; hexane; (under N2, Schlenk); ligand dissolved in Et2O, cooled to -78°C, Li-salt in hexane added dropwise, stirred for 2 h, warmed to room temp., SbCH3Cl2 added dropwise, stirred for 18 h, hydrolyzed with H2O; organics sepd., aq. soln. washed with Et2O, dried over MgSO4, filtered, volatiles removed under reduced pressure; elem. anal.;
DOI:10.1039/b909226a
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