Ph2B(μ-2,5-bis(2-pyridyl)-1,4-hydroquinone(2-))BPh2

Base Information

• Chemical Name: Ph2B(μ-2,5-bis(2-pyridyl)-1,4-hydroquinone(2-))BPh2
• CAS No.: 1191408-02-2
• Molecular Formula: C₄₀H₃₀B₂N₂O₂
• Molecular Weight: 592.312

Synonyms:

Chemical Property of Ph2B(μ-2,5-bis(2-pyridyl)-1,4-hydroquinone(2-))BPh2

Chemical Property:

Purity/Quality:

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Technology Process of Ph2B(μ-2,5-bis(2-pyridyl)-1,4-hydroquinone(2-))BPh2

There total 1 articles about Ph2B(μ-2,5-bis(2-pyridyl)-1,4-hydroquinone(2-))BPh2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

triphenylborane (960-71-4) + 2,5-bis(2-pyridyl)-1,4-hydroquinone → Ph2B(μ-2,5-bis(2-pyridyl)-1,4-hydroquinone(2-))BPh2 (1191408-02-2)

Guidance literature:

In tetrahydrofuran; (N2) soln. BPh3 in THF was added to soln. ligand in THF at room temp., react. mixt. was stirred overnight at room temp.; soln. was concd. in vacuo, petroleum ether was added, ppt. was filtered and purified by vac. sublimation; elem. anal.;

DOI:10.1021/ic900673s

upstream raw materials:

triphenylborane

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