1,2,4-triphenyl-cyclopentadienyltitanium trichloride

Base Information

Chemical Name:1,2,4-triphenyl-cyclopentadienyltitanium trichloride
CAS No.:913058-16-9
Molecular Formula:C₂₃H₁₇Cl₃Ti
Molecular Weight:447.627
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,4-triphenyl-cyclopentadienyltitanium trichloride

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Technology Process of 1,2,4-triphenyl-cyclopentadienyltitanium trichloride

There total 1 articles about 1,2,4-triphenyl-cyclopentadienyltitanium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.6%

: 5074-28-2
1,2,4-triphenyl-1,3-cyclopentadiene

: 7550-45-0
titanium tetrachloride

: 913058-16-9
1,2,4-triphenyl-cyclopentadienyltitanium trichloride

Guidance literature:: With n-BuLi; Me₃SiCl; In diethyl ether; hexane; (N2); to soln. of org. ligand in Et2O added n-BuLi in hexane at -78°C; room temp., overnight; solvent removed; Me3SiCl added to residue in THF at -78°C; 2 h, room temp.; residue in toluene added to TiCl4 at -78°C; 24 h, room temp.; precipitate filtered off; solvent removed; recrystallization in methylene chloride/n-hexane (1:3 v/v); elem. anal.;
DOI:10.1016/j.poly.2006.03.006