[[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) thiophenolate

Base Information

• Chemical Name: [[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) thiophenolate
• CAS No.: 1279725-58-4
• Molecular Formula: C₂₈H₄₄O₆P₂SSn
• Molecular Weight: 689.377
• Mol file: 1279725-58-4.mol

Synonyms:

Chemical Property of [[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) thiophenolate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) thiophenolate

There total 1 articles about [[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) thiophenolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

[[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) chloride + sodium thiophenolate (930-69-8) → [[2,6-bis(diisopropoxyphosphonyl)-4-tert-butyl]phenyl]tin(II) thiophenolate (1279725-58-4)

Guidance literature:

In tetrahydrofuran; byproducts: NaCl; NaSPh added to soln. (4-tBu-2,6-[P(O)(OiPr)2]2C6H2)SnCl (THF) at room temp.; stirred for 24 h; ppt. (NaCl) filtered; evap. solvents in vac.; recrystd. (toluene);;

DOI:10.1002/zaac.201000387

upstream raw materials:

sodium thiophenolate