1-butyl-1-methylpiperidinium hexafluorophosphate

Base Information

• Chemical Name: 1-butyl-1-methylpiperidinium hexafluorophosphate
• CAS No.: 1257647-66-7
• Molecular Formula: C₁₀H₂₂N*F₆P
• Molecular Weight: 301.256
• Mol file: 1257647-66-7.mol

Synonyms:

Chemical Property of 1-butyl-1-methylpiperidinium hexafluorophosphate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

1-Butyl-1-methylpiperidinium hexafluorophosphate 99% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1-Butyl-1-methylpiperidinium hexafluorophosphate (BMPIPPF6) is an ionic liquid that can be used to prepare modified carbon composite electrodes, which are used as sensors in the estimation of paracetamol, neurotransmitter drugs and NADH in the biological samples.

Technology Process of 1-butyl-1-methylpiperidinium hexafluorophosphate

There total 2 articles about 1-butyl-1-methylpiperidinium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

1-n-butyl-1-methylpiperidin-1-ium bromide (94280-72-5) → 1-butyl-1-methylpiperidinium hexafluorophosphate (1257647-66-7)

Guidance literature:

With potassium hexafluorophosphate; In dichloromethane; water; Flow reactor;

DOI:10.1016/j.tetlet.2021.153500

Reference yield:

1-Methylpyrrolidine (120-94-5) → 1-butyl-1-methylpiperidinium hexafluorophosphate (1257647-66-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 48 h / 65 °C / Inert atmosphere

2: potassium hexafluorophosphate / dichloromethane; water / Flow reactor

With potassium hexafluorophosphate; In dichloromethane; water; acetonitrile;

DOI:10.1016/j.tetlet.2021.153500

upstream raw materials:

1-Methylpyrrolidine

1-n-butyl-1-methylpiperidin-1-ium bromide