C₂₄H₂₉BNP

Base Information

• Chemical Name: C₂₄H₂₉BNP
• CAS No.: 1399049-71-8
• Molecular Formula: C₂₄H₂₉BNP
• Molecular Weight: 373.286
• Mol file: 1399049-71-8.mol

Synonyms:

Chemical Property of C₂₄H₂₉BNP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₄H₂₉BNP

There total 2 articles about C₂₄H₂₉BNP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

C22H23LiNP + methyllithium (917-54-4) → C24H29BNP (1399049-71-8)

Guidance literature:

C₂₂H₂₃LiNP; With boron trichloride; In diethyl ether; hexane; at -78 ℃;

methyllithium; In diethyl ether; hexane; at -78 - 20 ℃;

DOI:10.1002/hc.21033

Reference yield:

triphenylphosphine-N-tertbutylimine (13989-64-5) → C24H29BNP (1399049-71-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: methyllithium / diethyl ether / 2 h / 20 °C

2.1: boron trichloride / diethyl ether; hexane / -78 °C

2.2: -78 - 20 °C

With methyllithium; boron trichloride; In diethyl ether; hexane;

DOI:10.1002/hc.21033

upstream raw materials:

triphenylphosphine-N-tertbutylimine

methyllithium

Refernces