Boc-PheΨSta-Leu-NHCH2Ph

Base Information

Chemical Name:Boc-PheΨSta-Leu-NHCH2Ph
CAS No.:118404-95-8
Molecular Formula:C₃₈H₅₈N₄O₉
Molecular Weight:714.9
Hs Code.:

Boc-PheΨ<CHOHCHOHCHOHCONH>Sta-Leu-NHCH2Ph

Synonyms:

Suppliers and Price of Boc-PheΨSta-Leu-NHCH2Ph

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Boc-PheΨSta-Leu-NHCH2Ph

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Boc-PheΨSta-Leu-NHCH2Ph

There total 5 articles about Boc-PheΨSta-Leu-NHCH2Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118404-99-2,124338-96-1,124339-24-8
Boc-PheΨSta-Leu-NHCH2Ph

: 118404-95-8,124338-99-4,124339-27-1,124339-28-2,124339-29-3
Boc-PheΨSta-Leu-NHCH2Ph

Guidance literature:: With osmium(VIII) oxide; In tetrahydrofuran; 1,4-dioxane; for 96h; Ambient temperature;
DOI:10.1021/jm00164a058

Reference yield:

: 118457-05-9
Methyl (S)-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

: 118404-95-8,124338-99-4,124339-27-1,124339-28-2,124339-29-3
Boc-PheΨSta-Leu-NHCH2Ph

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature

2: 1.1 g / 1 N NaOH / methanol / 2 h / Ambient temperature

3: 325 mg / HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp., overnight

4: 430 mg / 2percent OsO₄ / tetrahydrofuran; dioxane / 96 h / Ambient temperature

With sodium hydroxide; osmium(VIII) oxide; benzotriazol-1-ol; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00164a058

Reference yield:

: 99113-32-3,99113-34-5,118386-98-4
(2E,4R,S,5S)-5-<<(1,1-dimethylethoxy)carbonyl>amino>-4-hydroxy-6-phenyl-2-hexenoic acid

: 118404-95-8,124338-99-4,124339-27-1,124339-28-2,124339-29-3
Boc-PheΨSta-Leu-NHCH2Ph

Guidance literature:: Multi-step reaction with 2 steps

1: 325 mg / HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp., overnight

2: 430 mg / 2percent OsO₄ / tetrahydrofuran; dioxane / 96 h / Ambient temperature

With osmium(VIII) oxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm00164a058