Technology Process of C56H76F6N2O15S2Si
There total 7 articles about C56H76F6N2O15S2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1039/c3cc42852d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonium hydroxide / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
3: lithium hydroxide / methanol; water; tetrahydrofuran / 1 h / 0 - 50 °C / Inert atmosphere
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere
5: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
With
ammonium hydroxide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42852d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium hydroxide / methanol; water; tetrahydrofuran / 1 h / 0 - 50 °C / Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere
3: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42852d