Technology Process of 3-(benzylthio)-N-phenethyl-3-phenylpropanamide
There total 3 articles about 3-(benzylthio)-N-phenethyl-3-phenylpropanamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; tetrabutylammomium bromide / toluene / 20 °C / Inert atmosphere
2: ytterbium(III) triflate / dichloromethane / 0 °C / Inert atmosphere
3: aluminum oxide / 4 h / 40 °C / Inert atmosphere
With
aluminum oxide; tetrabutylammomium bromide; ytterbium(III) triflate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane; toluene;
1: |Strecker Aminoacid Synthesis / 2: |Michael Addition;
DOI:10.1002/chem.201202291
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ytterbium(III) triflate / dichloromethane / 0 °C / Inert atmosphere
2: aluminum oxide / 4 h / 40 °C / Inert atmosphere
With
aluminum oxide; ytterbium(III) triflate;
In
dichloromethane;
1: |Michael Addition;
DOI:10.1002/chem.201202291
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; tetrabutylammomium bromide / toluene / 20 °C / Inert atmosphere
2: ytterbium(III) triflate / dichloromethane / 0 °C / Inert atmosphere
3: aluminum oxide / 4 h / 40 °C / Inert atmosphere
With
aluminum oxide; tetrabutylammomium bromide; ytterbium(III) triflate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane; toluene;
1: |Strecker Aminoacid Synthesis / 2: |Michael Addition;
DOI:10.1002/chem.201202291
