C₃₀H₂₇O₂P

Base Information

• Chemical Name: C₃₀H₂₇O₂P
• CAS No.: 1407182-89-1
• Molecular Formula: C₃₀H₂₇O₂P
• Molecular Weight: 450.517
• Mol file: 1407182-89-1.mol

Synonyms:

Chemical Property of C₃₀H₂₇O₂P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₇O₂P

There total 4 articles about C₃₀H₂₇O₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-(-)-1,1'-bi-2-naphthol triflate (128544-05-8,128575-34-8,141807-44-5,126613-06-7) → C30H27O2P (1407182-89-1,1407182-92-6)

Guidance literature:

Multi-step reaction with 3 steps

1: palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane / dimethyl sulfoxide / 16 h / 100 °C

2: sodium hydroxide / 1,4-dioxane; methanol / 18 h / 20 °C

3: potassium carbonate / acetone / 16 h / Reflux

With palladium diacetate; potassium carbonate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; sodium hydroxide; In 1,4-dioxane; methanol; dimethyl sulfoxide; acetone;

DOI:10.1016/j.tetlet.2012.07.136

Reference yield:

C30H24F3O4PS (1065271-81-9,1065271-82-0) → C30H27O2P (1407182-89-1,1407182-92-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / 1,4-dioxane; methanol / 18 h / 20 °C

2: potassium carbonate / acetone / 16 h / Reflux

With potassium carbonate; sodium hydroxide; In 1,4-dioxane; methanol; acetone;

DOI:10.1016/j.tetlet.2012.07.136

Reference yield:

(±)-isopropyl(phenyl)phosphine oxide (63762-20-9) → C30H27O2P (1407182-89-1,1407182-92-6)

Guidance literature:

Multi-step reaction with 3 steps

1: palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane / dimethyl sulfoxide / 16 h / 100 °C

2: sodium hydroxide / 1,4-dioxane; methanol / 18 h / 20 °C

3: potassium carbonate / acetone / 16 h / Reflux

With palladium diacetate; potassium carbonate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; sodium hydroxide; In 1,4-dioxane; methanol; dimethyl sulfoxide; acetone;

DOI:10.1016/j.tetlet.2012.07.136

upstream raw materials:

C₂₉H₂₅O₂P

methyl iodide

(R)-(-)-1,1'-bi-2-naphthol triflate

(±)-isopropyl(phenyl)phosphine oxide