C₂₅H₃₃N₃O₆

Base Information

Chemical Name:C₂₅H₃₃N₃O₆
CAS No.:1431768-49-8
Molecular Formula:C₂₅H₃₃N₃O₆
Molecular Weight:471.554
Hs Code.:

C<sub>25</sub>H<sub>33</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₅H₃₃N₃O₆

Chemical Property:

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Technology Process of C₂₅H₃₃N₃O₆

There total 10 articles about C₂₅H₃₃N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₄₁NO₃Si

: 1431768-49-8
C₂₅H₃₃N₃O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 7 h

2.1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / 7.67 h / -78 - 20 °C

3.1: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C

4.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 18.5 h / 0 - 20 °C

5.1: toluene / 13 h / Reflux

5.2: 1 h / 20 °C

6.1: triethylamine; pivaloyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

7.1: dichloromethane / 1.25 h / 0 - 20 °C

8.1: triethylamine / dichloromethane / 0 °C

With sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; pivaloyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol; 2.1: |Swern Oxidation / 5.1: |Curtius Rearrangement;
DOI:10.1021/jm4002296

Reference yield:

: C₂₄H₃₃NOSi

: 1431768-49-8
C₂₅H₃₃N₃O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / tetrahydrofuran / 27 h / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 7 h

3.1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / 7.67 h / -78 - 20 °C

4.1: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C

5.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 18.5 h / 0 - 20 °C

6.1: toluene / 13 h / Reflux

6.2: 1 h / 20 °C

7.1: triethylamine; pivaloyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

8.1: dichloromethane / 1.25 h / 0 - 20 °C

9.1: triethylamine / dichloromethane / 0 °C

With sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; pivaloyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol; 3.1: |Swern Oxidation / 6.1: |Curtius Rearrangement;
DOI:10.1021/jm4002296

Reference yield:

: C₁₃H₂₃NO₃

: 1431768-49-8
C₂₅H₃₃N₃O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / 7.67 h / -78 - 20 °C

2.1: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C

3.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 18.5 h / 0 - 20 °C

4.1: toluene / 13 h / Reflux

4.2: 1 h / 20 °C

5.1: triethylamine; pivaloyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

6.1: dichloromethane / 1.25 h / 0 - 20 °C

7.1: triethylamine / dichloromethane / 0 °C

With sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; pivaloyl chloride; triethylamine; In dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol; 1.1: |Swern Oxidation / 4.1: |Curtius Rearrangement;
DOI:10.1021/jm4002296