Technology Process of C23H26ClN3O3S*ClH
There total 9 articles about C23H26ClN3O3S*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere
1.2: 3 h / 20 °C / Inert atmosphere
2.1: hydroxylamine hydrochloride / ethanol / 6 h / Reflux
3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 4 h / 0 °C
4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 20 °C
5.1: tin(II) chloride dihdyrate / N,N-dimethyl-formamide / 20 °C
6.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 0.5 h
6.2: 48 h / 20 °C
7.1: hydrogenchloride / chloroform / 0.5 h / 0 °C
8.1: sodium cyanoborohydride / methanol / 24 h / 20 °C
9.1: hydrogenchloride / methanol / 0.5 h / 0 °C
With
hydrogenchloride; sodium tetrahydroborate; n-butyllithium; tin(II) chloride dihdyrate; di-isopropyl azodicarboxylate; hydroxylamine hydrochloride; sodium cyanoborohydride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; triphenylphosphine;
In
tetrahydrofuran; methanol; ethanol; hexane; chloroform; N,N-dimethyl-formamide;
4.1: Mitsunobu reaction;
DOI:10.1016/j.ejps.2010.11.010
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / chloroform / 0.5 h / 0 °C
2: sodium cyanoborohydride / methanol / 24 h / 20 °C
3: hydrogenchloride / methanol / 0.5 h / 0 °C
With
hydrogenchloride; sodium cyanoborohydride;
In
methanol; chloroform;
DOI:10.1016/j.ejps.2010.11.010
