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3-(3,5-Dibromophenyl)prop-2-enoic acid

Base Information Edit
  • Chemical Name:3-(3,5-Dibromophenyl)prop-2-enoic acid
  • CAS No.:202982-74-9
  • Molecular Formula:C9H6Br2O2
  • Molecular Weight:305.953
  • Hs Code.:
  • DSSTox Substance ID:DTXSID50695268
  • Mol file:202982-74-9.mol
3-(3,5-Dibromophenyl)prop-2-enoic acid

Synonyms:3-(3,5-Dibromophenyl)prop-2-enoic acid;DTXSID50695268

Suppliers and Price of 3-(3,5-Dibromophenyl)prop-2-enoic acid
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • Labseeker
  • 3,5-dibromocinnamicacid 95
  • 5g
  • $ 1228.00
  • Alichem
  • 3,5-Dibromocinnamicacid
  • 1g
  • $ 1519.80
Total 0 raw suppliers
Chemical Property of 3-(3,5-Dibromophenyl)prop-2-enoic acid Edit
Chemical Property:
  • XLogP3:3.3
  • Hydrogen Bond Donor Count:1
  • Hydrogen Bond Acceptor Count:2
  • Rotatable Bond Count:2
  • Exact Mass:305.87141
  • Heavy Atom Count:13
  • Complexity:206
Purity/Quality:

3,5-dibromocinnamicacid 95 *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
  • Canonical SMILES:C1=C(C=C(C=C1Br)Br)C=CC(=O)O
Technology Process of 3-(3,5-Dibromophenyl)prop-2-enoic acid

There total 6 articles about 3-(3,5-Dibromophenyl)prop-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium hydroxide monohydrate; In methanol; water; Reflux;
DOI:10.1016/j.bmc.2017.05.011
Guidance literature:
With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1039/c2cc35044k
Guidance literature:
Multi-step reaction with 2 steps
1.1: 18-crown-6 ether; potassium hexamethylsilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: 14.17 h / -78 °C / Inert atmosphere
2.1: water; lithium hydroxide / tetrahydrofuran / 4 h / 20 °C
With 18-crown-6 ether; water; potassium hexamethylsilazane; lithium hydroxide; In tetrahydrofuran;
DOI:10.1039/c2cc35044k
upstream raw materials:

malonic acid

3,5-dibromobenzaldehyde

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