[Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O

Base Information

Chemical Name:[Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O
CAS No.:452281-80-0
Molecular Formula:C₂₈H₂₉INP₂Pd*H₂O*I
Molecular Weight:819.737
Hs Code.:

[Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H<sub>2</sub>O

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Chemical Property of [Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O

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Technology Process of [Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O

There total 2 articles about [Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: sodium tetrachloropalladate(II)

: 7732-18-5
water

: 66534-97-2
bis(2-(diphenylphosphino)ethyl)amine hydrochloride

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 452281-80-0
[Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O

Guidance literature:: With NaCl; In dichloromethane; water; suspn. of Pd and Na compds. in water heated at 80°C, after dissolving cooled to room temp., soln. of org. compd. in CH2Cl2 added dropwise, stirred for 15 h at room temp.; org. phase extd. with CH2Cl2, dried with Na2SO4, filtered, solvent removed in vac., recrystd. from CH2Cl2-n-hexane, elem. anal.;
DOI:10.1039/b109675n

Reference yield: 71.0%

: 7732-18-5
water

: 66534-97-2
bis(2-(diphenylphosphino)ethyl)amine hydrochloride

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: palladium dichloride

: 452281-80-0
[Pd((bis(2-(diphenylphosphino)ethyl)amine)I]I*H₂O

Guidance literature:: With NaCl; In dichloromethane; water; suspn. of PdCl2 and 2 equiv. of NaCl in H2O heated at 80°C, 4 equiv. of powdered NaI added at room temp., CH2Cl2 soln. of 1 equiv. of P-compd. added dropwise, stirred at room temp. for 15 h; org. phase extd. with CH2Cl2, dried over Na2SO4, filtered, solvent was removed in vac., solid was recrystd. from CH2Cl2/n-hexane; elem. anal.;
DOI:10.1002/1521-3749(200206)628:5<1075::AID-ZAAC1075>3.0.CO;2-M