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C25H28N2O2

Base Information
  • Chemical Name:C25H28N2O2
  • CAS No.:877269-29-9
  • Molecular Formula:C25H28N2O2
  • Molecular Weight:388.51
  • Hs Code.:
C<sub>25</sub>H<sub>28</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C25H28N2O2
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Technology Process of C25H28N2O2

There total 8 articles about C25H28N2O2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With water; sodium hydroxide; In tetrahydrofuran; methanol; at 90 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1016/j.bmcl.2011.03.067
Guidance literature:
Multi-step reaction with 6 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / ethanol; toluene
2: sodium hydride / N,N-dimethyl-formamide / 20 °C
3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride
4: trifluoroacetic acid / dichloromethane
5: 10% palladium on activated charcoal; hydrogen
6: water; sodium hydroxide / tetrahydrofuran; methanol / 0.17 h / 90 °C / Microwave irradiation
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); 10% palladium on activated charcoal; water; hydrogen; sodium hydride; sodium carbonate; trifluoroacetic acid; lithium chloride; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.03.067
Guidance literature:
Multi-step reaction with 5 steps
1: sodium hydride / N,N-dimethyl-formamide / 20 °C
2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride
3: trifluoroacetic acid / dichloromethane
4: 10% palladium on activated charcoal; hydrogen
5: water; sodium hydroxide / tetrahydrofuran; methanol / 0.17 h / 90 °C / Microwave irradiation
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 10% palladium on activated charcoal; water; hydrogen; sodium hydride; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.03.067
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